A new tricyclic triketone from tandem condensation reactions

I. David Reingold, Anna M. Butterfield, Bevin C. Daglen, Robert S. Walters, Kathryn Allen, Susan Scheuring, Katrina Kratz, Milan Gembický, Peter Baran

Research output: Contribution to journalArticlepeer-review

7 Scopus citations

Abstract

Perhydrophenanthrene-1,5,10-trione (6) was isolated from the reaction of methyl 3-(carboxymethyl)cyclohexanone and cyclohexenone in a tandem Michael-Claisen reaction. NMR and X-ray analysis confirmed the structure of the product.

Original languageEnglish
Pages (from-to)3835-3837
Number of pages3
JournalTetrahedron Letters
Volume46
Issue number22
DOIs
StatePublished - 30 May 2005

Keywords

  • Claisen
  • Kekulene
  • Michael
  • Modeling
  • Perhydrophenanthrene
  • Tandem condensations
  • Tricyclic
  • Triketone

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