SPS Fabrication of Tungsten and Tungsten Rhenium Alloys in Support of NTR Fuels Development

Jonathan A. Webb, Indrajit Charit, Cory Sparks, Darryl P. Butt, Megan Frary, Mark Carroll

Research output: Chapter in Book/Report/Conference proceedingChapter

Abstract

Tungsten metal slugs were fabricated via Spark Plasma Sintering (SPS) of powdered metals at temperatures ranging from 1575 K to 1975 K and hold times of 5 minutes to 30 minutes, using powders with an average diameter of 7.8 µm. Sintered tungsten specimens were found to have relative densities ranging from 83% to 94% of the theoretical density for tungsten. Consolidated specimens were also tested for their Vickers Hardness Number (VHN), which were plotted as a function of relative density. Concurrently, tungsten and rhenium powders with average respective diameters of 0.5 µm and 13.3 µm were pre-processed either by High-Energy-Ball-Milling (HEBM) or by homogeneous mixing to yield W-25at.%Re mixtures. The powder batches were sintered at temperatures of 1975 K and 2175 K for hold times up to 60 minutes yielding relative densities in the range 94% to 97%. The combination of HEBM and sintering showed a significant decrease in the intermetallic phases compared to that of the homogenous mixing and sintering.

Original languageAmerican English
Title of host publicationNuclear and Emerging Technologies for Space 2011, NETS-2011, February 7-February 10, 2011, Albuquerque, NM
StatePublished - 7 Feb 2011

Keywords

  • Spark Plasma Sintering
  • nuclear propulsion
  • space reactors
  • tungsten alloys

EGS Disciplines

  • Materials Science and Engineering

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